Practical dissolution dynamic nuclear polarization


Elliott, Stuart J ORCID: 0000-0002-8726-0635, Stern, Quentin, Ceillier, Morgan, El Daraï, Théo, Cousin, Samuel F, Cala, Olivier and Jannin, Sami (2021) Practical dissolution dynamic nuclear polarization. Progress in Nuclear Magnetic Resonance Spectroscopy, 126-12. pp. 59-100.

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Abstract

This review article intends to provide insightful advice for dissolution-dynamic nuclear polarization in the form of a practical handbook. The goal is to aid research groups to effectively perform such experiments in their own laboratories. Previous review articles on this subject have covered a large number of useful topics including instrumentation, experimentation, theory, etc. The topics to be addressed here will include tips for sample preparation and for checking sample health; a checklist to correctly diagnose system faults and perform general maintenance; the necessary mechanical requirements regarding sample dissolution; and aids for accurate, fast and reliable polarization quantification. Herein, the challenges and limitations of each stage of a typical dissolution-dynamic nuclear polarization experiment are presented, with the focus being on how to quickly and simply overcome some of the limitations often encountered in the laboratory.

Item Type: Article
Uncontrolled Keywords: Magnetic Resonance Spectroscopy, Solubility
Divisions: Faculty of Science and Engineering > School of Physical Sciences
Depositing User: Symplectic Admin
Date Deposited: 10 Aug 2021 07:26
Last Modified: 18 Mar 2024 02:10
DOI: 10.1016/j.pnmrs.2021.04.002
Related URLs:
URI: https://livrepository.liverpool.ac.uk/id/eprint/3132995

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